DICHLOROMETHANE FOR LIQUID CHROMATOGRAPHY LICHROSOLV

Code: 1060449010 D2-231

Analysis Note

Purity (GC): ≥ 99.9 %Identity (IR): conformsAcidity: ≤ 0.0002 meq/gAlkalinity: ≤ 0.0002 meq/gTransmission (at 240 nm): ≥ 70 %Transmissio...


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€705.00 EACH
€867.15 inc. VAT

Analysis Note

Purity (GC): ≥ 99.9 %Identity (IR): conformsAcidity: ≤ 0.0002 meq/gAlkalinity: ≤ 0.0002 meq/gTransmission (at 240 nm): ≥ 70 %Transmission (at 245 nm): ≥ 90 %Transmission (from 260 nm): ≥ 99 %Evaporation residue: ≤ 5.0 mg/lWater: ≤ 0.01 %The product is stabilized with 2-Methyl-2-buten.Filtered by 0.2 µm filter

Application

Intended for HPLC and UHPLC-MS applications.

Features and Benefits

suitability tested and specified for UHPLC-MS and UHPLC-UV: for analytical flexibility specified quality in positive and negative in positive and negative electrospray ionization (ESI) and atmospheric-pressure chemical ionization-mass spectrometry (APCI-MS) for lowest detection limits and confidence in analyses for all important MS modes (test 1)R12;ESI/APCI (+) ﹤ 2 ppbR12;ESI/APCI (-) ﹤ 10 ppb lowest impurity profile: for interference-free baselines (test 2) microfiltered through 0.2 µm filter (test 3) to provide:R12;a long lifespan to filters and mechanical parts of HPLC systemsR12;reduced risk of column clogging packed in borosilicate glass bottles for minimum metal ion contaminations lowest levels of trace metal impurities for a minimum metal ion adduct formationR12;﹤ 5ppb lowest level of polyethylene glycol (PEG) impurities in UHPLC-MS solvent lineup (PEG S/N signal-to-noise-ratio ﹤ 50)

General description

LiChrosolv® solvents exhibit high degree of UV transmittance, low particle count, low acidity and alkalinity and low evaporation residue level. This makes them ideal for reproducible separations.

Legal Information

LICHROSOLV is a registered trademark of Merck KGaA, Darmstadt, Germany

Packaging

2.5, 4 l in Glass bottle

Preparation Note

Product filtered through a 0.2 µm filter

assay≥99.9% (GC)
autoignition temp.1223 °F, 605 °C (DIN 51794)
bp39.8-40 °C (lit.)
contains2-methyl-2-butene as stabilizer
density1.325 g/mL at 25 °C (lit.)
evapn. residue≤5.0 mg/L
expl. lim.22 %
formliquid
gradeisocratic
impurities≤0.01% Water, ≤0.0002 meq/g Alkalinity, ≤0.0002 meq/g Acidity
InChI keyYMWUJEATGCHHMB-UHFFFAOYSA-N
InChI1S/CH2Cl2/c2-1-3/h1H2
mp−97 °C (lit.), -95 °C
pH7 (20 °C)
potency>2000 mg/kg LD50, skin (Rat), 1600 mg/kg LD50, oral (Rat)
product lineLiChrosolv®
Quality Level100
refractive indexn20/D 1.424 (lit.)
SMILES stringClCCl
solubility20 g/L
storage temp.2-30°C
technique(s)HPLC: suitable
transmittance260 nm, ≥99%, 240 nm, ≥70%, 245 nm, ≥90%
vapor density2.9 (vs air)
vapor pressure6.83 psi ( 20 °C), 24.45 psi ( 55 °C)
Cas Number75-09-2
Hazard Class6.1
Un Number1593
Pack GroupIII
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